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Beilstein J. Org. Chem. 2013, 9, 486–495, doi:10.3762/bjoc.9.52
Graphical Abstract
Scheme 1: Asymmetric synthesis of 2-methyl-6-phenyl piperidine.
Scheme 2: (a) Davies amine, BuLi, THF, −78 °C; dr ≥ 94% ; (b) H2, Pd(OH)2, MeOH; (c) Na2CO3, PhCH2CO2Cl, CH2Cl...
Scheme 3: Modified synthetic route to15.
Scheme 4: Possible pathways to obtain phosphonate 13 (a) Davies amine, BuLi, THF, −78 °C; dr ≥ 95%; (b) H2, P...
Scheme 5: Synthesis of compound 14.
Scheme 6: General synthesis of compound 13 (a) Davies amine, BuLi, THF, −78 °C; (b) H2, Pd(OH)2/C, MeOH; (c) ...
Scheme 7: Optimization of conditions for the Horner–Wadsworth–Emmons reaction.